Synthesis of Dibromobis(triphenylphosphine)nickel (II)

To a beaker add 0.55 g of nickel(II) bromide trihydrate suspended in 10 mL of hot butanol and 1 g of triphenylphosphine in 4 mL of hot butanol with vigorous stirring. Then put the solution in a freezer to crystallize the product out.

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The solution

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Addition of the triphenylphosphine

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The pure product

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