Preparation of Tris(dibenzylideneacetone) dipalladium(0)

To 150ml of methanol dissolve 3.9 g of sodium acetate, 1.05 g of palladium(II) chloride and 4.6 g of dibenzylideneacetone while heating at 50°C. Stir for 4 h in 40°C and cool down to room temp, filter and wash with some water and acetone. Dry and recrystallize in benzene if needed.


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